| Publication type: | Article in scientific journal |
| Type of review: | Peer review (publication) |
| Title: | Stochastic temperature modulation : a new technique in temperature-modulated DSC |
| Authors: | Schawe, Jürgen E. K. Hütter, Thomas Heitz, Christoph Alig, Ingo Lellinger, Dirk |
| DOI: | 10.1016/j.tca.2006.01.031 |
| Published in: | Thermochimica Acta |
| Volume(Issue): | 446 |
| Issue: | 1-2 |
| Page(s): | 147 |
| Pages to: | 155 |
| Issue Date: | 2006 |
| Publisher / Ed. Institution: | Elsevier |
| Publisher / Ed. Institution: | Amsterdam |
| ISSN: | 0040-6031 1872-762X |
| Language: | English |
| Subjects: | IDP; DSC; Messtechnik |
| Subject (DDC): | 540: Chemistry |
| Abstract: | A new temperature-modulated differential scanning calorimetry (TMDSC) technique is introduced. The technique is based on stochastic temperature modulation and has been developed as a consequence of a generalized theory of a temperature-modulated DSC. The quasi-static heat capacity and the frequency-dependent complex heat capacity can be determined over a wide frequency range in one single measurement without further calibration. Furthermore, the reversing and non-reversing heat flows are determined directly from the measured data. Examples show the frequency dependence of the glass transition, the isothermal curing of thermosets and a solid–solid transition. |
| URI: | https://digitalcollection.zhaw.ch/handle/11475/4532 |
| Fulltext version: | Published version |
| License (according to publishing contract): | Licence according to publishing contract |
| Departement: | School of Engineering |
| Organisational Unit: | Institute of Data Analysis and Process Design (IDP) |
| Appears in collections: | Publikationen School of Engineering |
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Schawe, J. E. K., Hütter, T., Heitz, C., Alig, I., & Lellinger, D. (2006). Stochastic temperature modulation : a new technique in temperature-modulated DSC. Thermochimica Acta, 446(1-2), 147–155. https://doi.org/10.1016/j.tca.2006.01.031
Schawe, J.E.K. et al. (2006) ‘Stochastic temperature modulation : a new technique in temperature-modulated DSC’, Thermochimica Acta, 446(1-2), pp. 147–155. Available at: https://doi.org/10.1016/j.tca.2006.01.031.
J. E. K. Schawe, T. Hütter, C. Heitz, I. Alig, and D. Lellinger, “Stochastic temperature modulation : a new technique in temperature-modulated DSC,” Thermochimica Acta, vol. 446, no. 1-2, pp. 147–155, 2006, doi: 10.1016/j.tca.2006.01.031.
SCHAWE, Jürgen E. K., Thomas HÜTTER, Christoph HEITZ, Ingo ALIG und Dirk LELLINGER, 2006. Stochastic temperature modulation : a new technique in temperature-modulated DSC. Thermochimica Acta. 2006. Bd. 446, Nr. 1-2, S. 147–155. DOI 10.1016/j.tca.2006.01.031
Schawe, Jürgen E. K., Thomas Hütter, Christoph Heitz, Ingo Alig, and Dirk Lellinger. 2006. “Stochastic Temperature Modulation : A New Technique in Temperature-Modulated DSC.” Thermochimica Acta 446 (1-2): 147–55. https://doi.org/10.1016/j.tca.2006.01.031.
Schawe, Jürgen E. K., et al. “Stochastic Temperature Modulation : A New Technique in Temperature-Modulated DSC.” Thermochimica Acta, vol. 446, no. 1-2, 2006, pp. 147–55, https://doi.org/10.1016/j.tca.2006.01.031.
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