Title: A comparative study of the functionalization of mesoporous silica MCM-41 by deposition of 3-aminopropyltrimethoxysilane from toluene and from the vapor phase
Authors : Ritter, Hanna
Nieminen, Minna
Karppinen, Maarit
Brühwiler, Dominik
Published in : Microporous and Mesoporous Materials
Volume(Issue) : 121
Issue : 1-3
Pages : 79
Pages to: 83
Publisher / Ed. Institution : Elsevier
Issue Date: 2009
License (according to publishing contract) : Licence according to publishing contract
Type of review: Peer review (Publication)
Language : English
Subjects : ICBC; Mesopores; Functionalization
Subject (DDC) : 540: Chemistry
Abstract: The postsynthetic functionalization of mesoporous silica MCM-41 by vapor phase deposition of 3-aminopropyltrimethoxysilane is investigated as an alternative to the common practice of depositing from toluene. Particular emphasis is given to the possibility of eliminating the influence of trace water upon deposition from the vapor phase. The comparative study of samples prepared by different deposition methods requires identical degrees of functionalization. To obtain reliable information on the amount of surface-grafted aminopropyl groups, we have developed an analysis procedure based on the fluorogenic amine-derivatization reaction of fluorescamine.
Departement: Life Sciences und Facility Management
Organisational Unit: Institute of Chemistry and Biotechnology (ICBT)
Publication type: Article in scientific Journal
DOI : 10.1016/j.micromeso.2009.01.006
10.5167/uzh-17901
ISSN: 1387-1811
URI: https://digitalcollection.zhaw.ch/handle/11475/2930
Appears in Collections:Publikationen Life Sciences und Facility Management

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